The effect of temperature on the 29Si magic angle spinning n.m.r. spectrum of highly siliceous ZSM-5

Colin A. Fyfe; Gordon J. Kennedy; George T. Kokotailo; James R. Lyerla; William W. Fleming

doi:10.1039/c39850000740

Journal of the Chemical Society, Chemical Communications

Paper

01 Jan 1985

The effect of temperature on the ²⁹Si magic angle spinning n.m.r. spectrum of highly siliceous ZSM-5

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Abstract

29Si magic angle spinning n.m.r experiments on highly siliceous ZSM-5 have shown that there is a phase transition in the temperature range 295-363 K in agreement with the results of powder X-ray diffraction measurements.

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